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Research on the Control Index of High Mass Concentration Flowback Fluid in Chengdao Oilfield
Lü Jiaxing, Hou Lei, Liu Fangyuan, Zhu Zhenyu, Wang Yujiang
Abstract303)   HTML    PDF (904KB)(55)      
The flowback fluid during oil acidizing operation process would directly enter the gathering and transportation system,resulting in deterioration or invalidation of conventional treatment agents,such as demulsifiers.The flowback fluids from the Chengdao Oilfield were divided into two types ,one is high mass concentration,the other is low mass concentration.The high mass concentration flowback fluid is transported back by the operating ships to the shore for further treatment,and the low mass concentration flowback fluid is directly discharged into the gathering and transportation system under the ground.The flowback cycle is long and affected by sea conditions. In order to reasonably estimate the amount of high mass concentration flowback fluid produced by crude oil dehydration process,this paper analyzes the factors affecting the oil⁃water separation of acidified flowback fluid.The volume of flowback fluid and indicators of water in two acidified oil wells were monitored,and thermal deposition of mixed flowback fluid and crude oil were tested. According to the demulsification effect and the water content of crude oil form the joint station, the quantified critical control index are listed as: the pH value of the water from the acidified oil well is higher than 6, the iron ion concentration is lower than 250 mg/L;and the auxiliary control index: the amount of backflow reaches 6 times higher than that of the acid liquid. An inspection method is proposed for the on⁃site operation of the flowback fluid discharging into the gathering and transportation system, properly reducing the flowback time without adding a new processing flow, which is beneficial to increase the oil well production rate and improve economic efficiency.
2021, 34 (1): 34-38. DOI: 10.3969/j.issn.1006-396X.2021.01.006
Effect of Physicochemical Conditions on the Stabilization of Shengli Crude Oil Emulsion
Yang Fengbin, Wang Yujiang, Zhang Lei, Zhang Lu
Abstract408)      PDF (2894KB)(216)      
The stability of emulsion of Shengli crude oil and variation of drop size were investigated using LUMisizer-LS610. At the same time, the influences of the emulsifier concentration,the wateroil ratio, temperature and electrolyte on the stability of emulsion and the drop size were also explored. The results show that the higher emulsifier concentration is, the smaller the drop size would be and the more stable crude oil emulsion is. The greater the proportion of oil phase in emulsion, the more stable the emulsion is. As the temperature increases, the good emulsified effect is obtained, however, the stability of the emulsion is reduced. The electrolyte can enhance the stability of the emulsion and reduce the drop size.
2017, 30 (6): 26-31. DOI: :10.3969/j.issn.1006-396X.2017.06.006
Preperation and Hydrodearomatization Performance of NiWP Catalyst Containing Hierarchical H β
Wang Yujia, Yue Yuan, Lu Cong, Wei Min
Abstract344)      PDF (2437KB)(84)      
 

The hierarchically mesoporous Hβ zeolite was synthesized by alkali treatment to commercial Hβ zeolite in NaOH solution. The composite carrier was prepared by mixing the hierarchical Hβ zeolite and Al2O3.The hierarchical NiWP/HβAl2O3 catalysts were prepared by incipient wetness impregnation method, and characterized by means of XRD, BET and TEM. The hydrodearomatization of the prepared NiWP/HβAl2O3 catalyst was evaluated in a miniature fixed bed reactor with fluid catalytic cracking diesel as raw material. The results suggested that the prepared NiWP/HβAl2O3 catalyst has an excellent hydrodearomatization activity, and under the condition of the reaction temperature 360 , reaction pressure 8.0 MPa, hydrogen to oil volumetric ratio 800 and liquid hourly space velocity 1.0 h-1, the cetane number was increased from 7.21 of feed to 46.96 of product.

2016, 29 (2): 13-17. DOI: 10.3969/j.issn.1006-396X.2016.02.003